Synthesis and Structural Properties of Nanoselenium-Supported MCM-41 Material


Yusof A. M. , YUŞAN S.

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, cilt.46, ss.747-753, 2016 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 46 Konu: 5
  • Basım Tarihi: 2016
  • Doi Numarası: 10.1080/15533174.2014.989579
  • Dergi Adı: SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY
  • Sayfa Sayısı: ss.747-753

Özet

The authors describe herein a new process for the synthesis of nanoselenium-supported MCM-41 hybrid material. Selenium nanoparticles were synthesized via chemical reduction method that this method is capable of producing spherical selenium nanoparticles of size 20 to 80nm, under ambient conditions, and covalently bonded to MCM-41 framework by 3-(triethoxysilyl)-propylamine (APTES). The structures, morphology and size of the products were investigated by several characterization techniques such as XRD, SEM, TEM, FT-IR, UV-vis/DRS, Raman spectroscopy, and N-2 adsorption-desorption isotherms method. These results demonstrated that Se-MCM-41 is a promising candidate for biosensor, adsorbent, or catalyst.